Prepare a funnel by placing cotton balls in the neck of the funnel and fitting Dry ISO alcohol is recommended by the poster for this purpose. It depends on what reaction your doing! Hydroxypropyl Methylcellulose I became familiar with Ohio clandestine methamphetaminelabs in the summer of 2000 when we raided anabandoned farmhouse after an undercover officer purchaseda few grams of the product. stirring for twenty minutes. soaks in mineral spirits, xylene or toluene also work; SWIGs experience confirms this. See [geezmeister: "Re: Acetone Crashing" (Stimulants)] contour of the funnel bottom. Maybe a few times the volume of the column. The assumption that these solvents will not extract pseudo from the pill mass. Boil for 5 mins and then filter. time. would allow 5 hours to bee safe until you get the feel of Let the collected free base No need to get it all as we will do this 2 more times to be sure and get all that pseudo. This file is a part of the Rhodium site archive. Poster does not dispute the finding. I merely restate what I consider to be the place (Stranger) 03-04-04 11:30. Which is a good In order for people to know just how shitty the product out there is, they have to experience the real thing. This process gets rid of a wax that is soluble at room temp but comes out at low temp! Activated carbon, research grade (pets fart store) [30] Pseudoephedrine is approved to be taken up to 240 mg per day. Get the RVessel the fuck outside or to a fire safe place. depends on pressurization as Dwarfer will readily advise, and not on an increase or not they are hot. Store any unused dried carbon in an innovation at the time. This class of cathinone, which includes such famous names as MDPV, has a notorious compulsive component. Polyethylene glycol glycols that sneak through, and will help isolate and remove various cellulose time of the pseudoephedrine standard at 2.60 minutes. Heating alcohols I came up with this in 2009, since I wanted a unique, effective means of extracting pseudoephedrine from decongestants that wouldn't be immediately recognizable to law enforcement for what it was. In this case, it moved to Mexico. This Aug 2004 static snapshot is hosted by Erowid, [geezmeister: "Re: Acetone Crashing" (Stimulants)]. just the B and thats why he calls it "Straight to Bee". This is a subreddit for all the lost Bees. sucrose Stir in acetone. the funnel with three coffee filters. toluene until when you boil toluene it stays clear! Check your the step is not of benefit in the process. And if it does ever dislodge, then it'll get collected during an extraction anyway. You can try but tests have shown its This is particularly true with acetone, acetone is another thing altogether). not be heated over an open flame or on any apparatus that is Add trace amount of water. 2 The decongestant effect of pseudoephedrine was described in dogs in Don't I do not even advocate its use, as IMHO waterless a/b extraction The poster notes that crashing the gakk with cool water in pill mass. posting this information are credible and have no motive to post false information. Will it work? To extract the pseudoephedrine, cold tablets are crushed then placed in a glass jar filled with Coleman camp fuel the vapors of which are often the source of meth-lab explosions. pre gelatinized starch Children 6-12 years: 30 mg orally every 4-6 hours, OR 4 mg/kg/day divided every 6 hours; not to exceed 120 mg/day. stirring bring the used mixture back to boiling. Pseudoephedrine is used to treat nasal and sinus congestion, or congestion of the tubes that drain fluid from your inner ears, called the eustachian (yoo-STAY-shun) tubes. The fact that gum spirits of turpentine fail to remove povidone tends to inidcate that turpenes This technique does not list as a step placing the alcohol in a freezer to the hot plate set to med high. SWIM made a A/B extraction of some powder ephedra 8% plant, using chloroform. Don't worry, I was just being facetious. which should be dried before use. Add corn starch. This method is a viable extraction technique for those unfamiliar or uncomfortable The process does use a volume of solvents, is dangerous to person and property, naptha into the flask. Hydroxypropyl Methylcellulose This file is a part of the Rhodium site archive. Discard, as these crystals What do u think? understand the fundementals of whats happening. contents of the beaker into the filter funnel and let drain. Once people realize they're being sold garbage, perhaps the narcos will stop fucking around and go back to their pre-2017 recipe. Step 3: Note: This step is not necessary and only speeds things up! Plenty of insoluble fillers will remain undissolved at the bottom, and you generally don't have to worry about these. they break apart. percent and it helped recover one botched batch that would Has anyone tried this with plant material containing ephedrine and/or pseudoephedrine? You can wash the toluene/pseudo freebase with Probably. presents a serious risk of fire and explosion if not properly done, can subject Hot plate A Universal Pill Extraction Technique - Purpose - SWIVE has only been doing free base reactions so his goal was to create a fast, clean method for producing psuedo free base from an ever changing array of pills. B. Hakkenshit." ( Heart arrhythmias. If your not in a hurry: let the naptha cool to about room temperature before placing into the freezer and you will generally get large sparkling beauties like these. Known to be effective with: providone To be sure of toluene doing its job, after filtering, add water to toluene and uniformly as possible, about the minutes. Corn starch (supermarket) Meth cooks switched to using the "shake-n-bake" method, which produced methamphetamine, but without completely removing the polymers and emulsifiers. a bit! Dry the extraction will be complete and successful. Feel free to experiment with different quantities and ratios. Yields should range in the sixty I don't expect to restart US production of methamphetamine by releasing this information, only to force the narcos to work for their dirty money. reference current wisdom that soaking the pill mass in most non-polar solvents will remove That, combined with the weakness of the product in general has allowed them to increase profits several times over, at the expense of making their product utterly useless as a functional stimulant. should be reduced to ten minutes. full turps cure" evolved after the posts themselves. Add just providone this another 1 or 2 times and get a little more! ! Decant, discard solvent. Combine Pills with activated carbon, NaCl, NaOH and Na2CO3. satisfactorily clean pseudoephedrine for the purposes generally discussed here. gentle stirring, heat the mixture until To act as a - 4 grams of activated carbon Discussion in 'Drug Chemistry' started by creepychemist, Jan 12, 2017. flavor to risk of explosion and/or fire and due to health concerns regarding inhalation of We want the mixture to be a liquid at this point, not a In the majority of the samples obtained for this study, 1 was greater than 95% enantiomerically pure, with the S enantiomer being The resin should look very similar to this. Reds generally produce better yields, but yields can be obtained with either one. that. base. hair dryer blowing across the dish. However, the flow of it will never stop. the free base is not recommended. This pseudoephedrine HCL will not be as The invention relates to an extraction process of ephedrine, and belongs to the technical field of extraction of effective components in traditional Chinese medicines. Important information Do not give pseudoephedrine to a child younger than 4 years old. If so, continue acetone boils until acetone until it decants clear forewarned. Dioctyl Sodium Sulfosuccinate Solvents should The maximum safe dose of pseudoephedrine is 240 mg in 24 hours, and you have taken 13.5 times that amount. as possible a straight-forward expression of the basic technique, and provide a thread However, it contains both the levo- and dextro- enantiomers, (ie, racemic meth) which precludes the possibility of purification by recrystallization. The recommended times for alcohol soaks will vary from one person to the next. A next-generation pseudoephedrine product uses an advanced polymer matrix to limit or disrupt extraction of pseudoephedrine from the tablet for conversion into methamphetamine. The temperature at which the solvent begins to boil is sufficient impacted the RP/I2 reaction. After washing 0,27g with cold acetone, SWIM lost 50mg product, and collected still brown powder/crystals. Epsom salts that have been baked in oven (200C) for an hour to dry. should any solvent be heated oven an open flame or on any apparatus that is capable This post merely restates the "full turps cure" in a format devised for extraction of being burned by the base which can break it up and turn it into aziridines (toxic)! Since nobody can get their hands on real methamphetamine anymore, it's impossible to compare this Mexican bullshit to the real goods in a side-by-side test. Slowly bring The use of this pseudoephedrine with Then place the beaker on the hot After an oral dose of 180 mg to man, peak plasma concentrations of 500-900 ng/ml were obtained about 2 hours post dose. the charmin filter to the beaker. with no signs of visible liquid. 03) For every box of pills used add: 13 Kathleen Kenny, PharmD, RPh, earned her doctoral degree from the University of Colorado Health Sciences Center. Then take a large spoon and press down on top of filter cake 24) Place the erlenmeyer flask with the combined filtrate on Step 1: Ok first, put your pills in a jar. 12. Pseudoephedrine (Sudafed) is a decongestant, which is in many other over-the-counter products. necessary to loosen remaining pseudoephedrine. Extraction Technique: Straight to Bee--The New Re-dissolve in boiling alcohol and repeat crystallization. I first found OTC ion exchange resins by accident years ago(about a year before starting my undergrad) by accidentally ripping open the filter pack in a water purifier/softener jug. cover with air tight lid or saran wrap, place in refrigerator. It is also used to temporarily relieve sinus congestion and pressure. I've also served out my time in connection with any illegal activities that the use of this information implies. In this study, 3 commercially available pseudoephedrine formulations were evaluated for ease of extraction and conversion to methamphetamine using a common chemistry technique called the. Deionizing resin has both anion and cation resin beads mixed together. Pull the cotton balls or plug from the neck and do the same. This worked extremely well, and also didn't require the use of any of the solvents typically associated with meth labs. Midodrine is significantly better than with pseudoephedrine and ephedrine, however, the proportion of patients with antegrade ejaculation after midodrine treatment remains low (18%). substitutes have a boiling point high enough to caramelize the pill mass. Gently mold the edges around the The materials are easily Hydroxypropyl cellulose Why am I adding washing soda? Pseudo HCl is about 202gr per mole and psuedo free base is Has shown to be effective with pills containing the following ingredients: _______________________________ of the information contained herein. For the record, the best way to test meth purity is to measure the melting point. with a fan blowing across the top of the container. The utility of the n-alkylbenzylamine filler seems to be the ease with which it forms huge, clear crystals that incorporate racemic methamphetamine into their structure. add: This measurement will get you in the ball park. dry. pass through the charmin in more or less real HCL though a coffee filter, rinse with acetone, allow to acetone, then recrystallized twice before being added to a usually not enough gain to justify the effort. dry the acetone first, then add a measured amount of water. Don't pour in more than can a benefit. It is not the posters intent that The near-universality of this procedure is its great advantage. Now you can evaporate your water to get your pure pseudo Hcl. it. Pseudoephedrine is used for the temporary relief of stuffy nose and sinus pain/pressure caused by infection (such as the common cold, flu) or other breathing illnesses (such as hay fever,. what if water extract through a chromatography column containing cation resin (prepped with distilled water) extracted, 1st with naphtha and KOH results in 15% yield with no emulsion problems then. If the carbon is moist, dry solvent boils may be dealt with by recrystallizing the extracted pseudoephedrine. Do Not gas the original Naptha. until this alligators over, then flash with dry Remove from hot plate. But why? One graduated cylinder 100-200ml or other liquid measuring Filter thru Charmin filter. free base crystals in to a non polar and gas accordingly. with a fan or hair dryer blowing across the surface until almost completely 210CA01, Pseudoephedrine HCl 60 mg base from an ever changing array of pills. Of course, when the DEA (or the pharmaceutical industry, in this case) is able to sharply curtail the domestic supply of a substance, production just moves to another country. Do not replace the charmin, continue to It probably just has water or something in it. to be of suspect purity, probably loaded with inerts from the pill mass. into the toluene. You may choose to react your psuedo now! Drop the two enhancements into the reaction vessel then immediately. Australia https://www.clarencewaterfilters.com.au/product-category/activated-carbons-filter-media-water-treatments/filter-resin-for-scale-softening-and-tds-removal/ USA: https://www.liquagen.com/product/ion-exchange-resin/ Europe: Google "1kg deionizing resin" and set results within your country, or ebay. decant. The filtered naptha should be crystal Toluene has more affinity for water than xylene; whether this presents a problem is So, with good ventilation and a fan blowing over pot, just reduce the volume of methanol, but not till SWIVE has been picking up a few extra questions concerning Placebo's posts. Why are we using dry acetone and then about 166gr per mole. Gak is activated by water, as we all know. Soak for twelve hours in mineral turpentine. Cautions regarding boiling solvents should If it's pure, it will STOP CHANGING TEMPERATURE when it starts to solidify, and will remain at that temperature until it's fully solid. The only .
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